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Smoltek Hydrogenated AGC at the Smoltek office

Smoltek Hydrogen has finalized design of a Prototype Coater tool for carbon nanofibers

Smoltek Hydrogen and AGC Plasma Technology Solutions have finalized the design of a Prototype Coater for industrial growth of carbon nanofibers. The purpose with the tool is to verify that the nanofibers can be grown using a Plasma Enhanced Chemical Vapor Deposition (PECVD) technology from AGC. The technology is scalable and can be extended to be used for substrates of several square meters, for future mass production.

May 28, 2024

Smol­tek Hydro­gen is work­ing on solv­ing the biggest pain point of PEM elec­tro­lyz­ers – “The Iridi­um prob­lem”. Iridi­um is needed as cata­lyst on the anode side in an elec­tro­lyz­er cell. How­ever, iridi­um is extremely expens­ive and most of all scarce and a lim­ited resource, and the short­age of iridi­um is recog­nized as the single most severe threat towards scal­ing up PEM elec­tro­lyz­ers. For this reas­on, the hydro­gen industry is eager to find a new, game-chan­ging tech­no­logy that can sig­ni­fic­antly reduce the iridi­um load. 

Smol­tek Hydro­gen has a solu­tion to this par­tic­u­lar prob­lem, by intro­du­cing an ultra-thin iridi­um coat­ing on the por­ous trans­port lay­er side instead of the mem­brane, and where the sur­face area first has been enlarged by coat­ing the sur­face with cor­ro­sion pro­tec­ted ver­tic­al car­bon nan­ofibers.
Smol­tek Hydro­gen aims to reduce the iridi­um amount with 95% com­pared to today’s stand­ard mater­i­al (that uses ca 2.5 mg iridium/​cm2), and has recently com­pleted a 1,000 hour dur­ab­il­ity test with only 0.2 mg iridium/​cm2 (Read about the test).

Man­u­fac­tur­ing tech­no­lo­gies to enable scale-up of PEM elec­tro­lyz­ers
Besides hav­ing a game chan­ging tech­no­logy, Smol­tek Hydro­gen also need to be able to man­u­fac­ture the elec­tro­lyz­er cell mater­i­al in large volumes. Today the samples are pro­duced with labor­at­ory tech­no­lo­gies, in low quant­it­ies and with typ­ic­al area of only a few square cen­ti­meters, where­as the indus­tri­al man­u­fac­tur­ing concept must be scal­able to the high volumes fore­seen, which is tens of thou­sands of square meters a year, and beyond. 

An import­ant first step towards indus­tri­al­iz­a­tion and com­mer­cial­iz­a­tion of the Smol­tek Hydro­gen elec­tro­lyz­er cell mater­i­al is prac­tic­al val­id­a­tion of the selec­ted concept for the growth of nan­ofibers, since it is a dif­fer­ent type of Plasma Enhanced Chem­ic­al Vapor Depos­ition (PECVD) pro­cess than used today. In order to do this Smol­tek Hydro­gen has, togeth­er with AGC Plasma Tech­no­logy Solu­tions, designed a new ded­ic­ated Pro­to­type Coat­er tool that will be placed in the Chalmers MC2 facil­it­ies in Gothen­burg, where Smol­tek cur­rently has its nan­ofiber fab­ric­a­tion operations.

Smoltek Agc Tool Design
Ilus­tra­tion of the Pro­to­type Coat­er which has been designed in col­lab­or­a­tion with AGC Plasma Tech­no­logy Solu­tions. The Pro­to­type Coat­er shall be used to val­id­ate the scal­able high-volume man­u­fac­tur­ing tech­no­logy for growth of car­bon nanofibers.

The Pro­to­type Coat­er is a power­ful tool with small foot­print and will provide an import­ant plat­form for con­tin­ued devel­op­ment of indus­tri­al growth recipes. The ambi­tion with the tool is to com­bine scal­able AGC lin­ear hol­low cath­ode PECVD tech­no­logy and our expert­ise in grow­ing car­bon nan­ofibers. We fine tune dif­fer­ent growth con­di­tions and select the para­met­ers most suit­able for fur­ther scale-up. The tool will also enable us to man­u­fac­ture rep­res­ent­at­ive samples to cus­tom­ers with indus­tri­al scal­able technology.

Shafiq Kabir, Head of Volume Pro­cesses at Smol­tek Hydrogen

Based on the learn­ings from val­id­a­tion of the Pro­to­type Coat­er, Smol­tek Hydro­gen aims to order a Pilot Coat­er, which is a smal­ler ver­sion of a high-volume tool. This is also a cru­cial com­pon­ent of AGC’s busi­ness mod­el, since they guar­an­tee the per­form­ance of the volume machine if their smal­ler coat­er is used to spe­cify its require­ments. The Pilot Coat­er will be used to pro­duce test series for cus­tom­ers as well as for veri­fic­a­tion of the pro­duc­tion tech­no­lo­gies before volume manufacturing.

Smoltek Manufacturing Strategy 2024 04
The roadmap for scal­ing up pro­duc­tion of Smol­tek Elec­tro­lyz­er Cell Mater­i­al is per­formed in sev­er­al phases. The val­id­a­tion of the selec­ted concept for the growth of nan­ofibers in the Pro­to­type Coat­er is an import­ant first step in the indus­tri­al­iz­a­tion & com­mer­cial­iz­a­tion phase.

About AGC
AGC Plasma Tech­no­logy Solu­tions is a new busi­ness unit with­in AGC Glass Europe SA, a European lead­er in flat glass. AGC Plasma Tech­no­logy Solu­tions is provid­ing low-pres­sure plasma coat­ing tech­no­logy and equip­ment. AGC Plasma is an expans­ive team of plasma coat­ing experts spe­cial­ized in innov­at­ive PVD and PECVD applic­a­tions from R&D and new product devel­op­ment all the way through to equip­ment man­u­fac­tur­ing and oper­a­tion­al man­age­ment of mass pro­duc­tion coat­ing plants. Vis­it the web­site www.agc-plasma.com to learn more about the equip­ment and ser­vices offered by AGC Plasma Tech­no­logy Solutions.

People pic­tured in the top photo, from left: Amin Saleeem, Bas­tien Pen­ninckx, Shafik Kabir, Erwan-Axel Mor­ris­son (AGC), Fabi­an Wenger, Jer­oen Schot­saert (AGC), Ellinor Ehrn­berg, Réka Simon-Balint.

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